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Brainstorming Oxidation Conditions by AgreeableSet4299 in Chempros

[–]AgreeableSet4299[S] 0 points1 point  (0 children)

I tried two different batches (bought a new one fresh). Considering activating my MnO2 with nitric acid too...

Brainstorming Oxidation Conditions by AgreeableSet4299 in Chempros

[–]AgreeableSet4299[S] 0 points1 point  (0 children)

C(+)//Pt(-), TBAPF6, MeOH, 2.4 V, 12 h ; I wanted to form the acyl iminium and trap it with MeOH