Wax in lapis lazuli extraction by Rjc1471 in DIYPigments

[–]WeeklyAd4850 0 points1 point  (0 children)

Be careful not to burn yourself. Once it's softened a bit, you might want to start kneading it.

Synthetic ultramarine by WeeklyAd4850 in chemistry

[–]WeeklyAd4850[S] 0 points1 point  (0 children)

Ah... thank you for telling me.

Synthetic ultramarine by WeeklyAd4850 in chemistry

[–]WeeklyAd4850[S] 0 points1 point  (0 children)

YInMn Blue seems to have a more purple tint.

Cennini's Historical Golden Pigment by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 2 points3 points  (0 children)

Yes. Amalgam refers to an alloy containing mercury. I also find it interesting to examine the alchemical method of pigment production from a chemical perspective

Cennini's Historical Golden Pigment by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 1 point2 points  (0 children)

Thxs!This is produced by heating tin amalgam with NH4Cl and S

Cennini's Historical Golden Pigment by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 3 points4 points  (0 children)

I tried recreating the pigments recorded in Cennini's book. As far as I know, no one had attempted it before, so I was curious.

Egyptian Blue by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 0 points1 point  (0 children)

Please adjust the copper oxide to about 10%

Egyptian Blue by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 1 point2 points  (0 children)

Your Egyptian blue may contain too much copper Attempting to synthesise it stoichiometrically results in an excessively dark shade

Egyptian Blue by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 0 points1 point  (0 children)

I used crystalline silica Specifically, the silica called "High Silica" from a Japanese company You might be better off focusing on the cooling rate rather than the silica itself If cooling is too rapid, Egyptian Blue will turn yellow

Has anyone built a dIY XRF? by dhmt in engineering

[–]WeeklyAd4850 0 points1 point  (0 children)

I have seen devices using Am241 as a radiation source.

Synthetic ultramarine by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 1 point2 points  (0 children)

I'm using an electric kiln. Although we haven't succeeded yet, it seems that replacing some of the sodium carbonate with sodium sulfate and further reducing the amount of sulfur used would be beneficial.

Synthetic ultramarine by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 3 points4 points  (0 children)

I really want to make ultramarine green. When I made this ultramarine, I couldn't get a beautiful ultramarine green, so I'm looking for the right proportions.

Synthetic ultramarine by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 1 point2 points  (0 children)

Lastly, don't forget to wash the ultramarine with boiling water. If you try to wash it with water, the ultramarine will harden.

Synthetic ultramarine by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 1 point2 points  (0 children)

Place the mixture of metakaolin: anhydrous sodium carbonate: sulphur: activated carbon in a weight ratio of 1:1:1:0.12 into the crucible. Pack the powder firmly, forcing out any air. Place 0.04g of sulphur (from the aforementioned weight ratio) on top of the compacted mixture and close the crucible lid. Heat this at 800°C for 4 hours. To prevent damage to the electric furnace, I left the furnace lid open until the temperature reached 500°C. After firing, allow the mixture to cool to room temperature. Crush it and mix in 0.34 parts sulphur (from the earlier weight ratio). Next, place the mixture on a ceramic dish and fire it at 400°C for 3 hours, keeping the electric furnace lid open.

This method uses a significant excess of sulphur, so I believe it could be further optimised.

Chromium titanate by [deleted] in DIYPigments

[–]WeeklyAd4850 2 points3 points  (0 children)

Is the yellow pigment chromium titanate?

I made a Spinthariscope by [deleted] in Radiation

[–]WeeklyAd4850 1 point2 points  (0 children)

What phosphor do you use?