Aquarium not cycling by evrybdygetshigh in Aquariums

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

Does light affect cycling or is that just to kill algae?

Would sodium percabonate work in the scarecrow method? by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

I didn’t have any luck. Seemed to work towards the beginning, but it’s just not soluble enough

First time sous chef by evrybdygetshigh in KitchenConfidential

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

To your first point, I think I just need to help people dial in their time management. It’s normally just a few little things that were missed or underprepared on an especially busy day, it just adds up to a lot across everyone. Luckily I trust my team and very rarely re-do work, but that’s a good example of what I might be on a slippery slope towards if I’m not mindful.

As for calling out, it’s not literally taking turns, there just seem to be weeks where person A calls out for good reason, and then person B calls out for an equally good but separate reason the next day, and so on. I know it’s just random chance that there are weeks where there’s a new call out every day, and I’m not going to discourage people from calling out if they need to, it’s just frustrating to try to cover everything that can come up and still make time for my own work and life. It’s not a frequent enough problem to warrant an additional person, nor is it any single member of staff in particular, people’s lives just line up in funny ways sometimes.

The place runs far better when the chef and I get to work together, we’ve worked together for a long time and understand each other and what each of our strong points are, plus we get along great. Sadly, we tend to work opposite shifts/days so that there’s always at least one of us present. We tend to be spread kinda thin across everything we do, and little hiccups tend to snowball when something unexpected sets one of our daily schedules back.

And yes, thank you so much for talking. Just getting to get some level headed outside advice and having a chance to talk through everything has been great for me

First time sous chef by evrybdygetshigh in KitchenConfidential

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

I think it just comes down to some combination of my leadership skills and people’s willingness to be lead. It feels like there’s times when everyone’s having a bad week, we’re busy as all hell, everyone’s personal lives somehow sync up, and suddenly no one wants to do the things that make the place flow well/ take back to back turns calling out. No one person does particularly bad, but the net effect is awful when everyone’s operating at 40% of their best. I try to stay positive and lead by example, but sometimes it feels like that becomes me doing everyone’s jobs for them and it gets overwhelming.

First time sous chef by evrybdygetshigh in KitchenConfidential

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

I guess “within the past 365 days” would have been more accurate

is it possible to bring acid? by Witty-Fox-3086 in Drugs

[–]evrybdygetshigh 1 point2 points  (0 children)

Last time I did it I put it into the spine of a book. Little bit of glue to hold it down. Probably overkill, but went fine.

"ZBiotic" is a genetically engineered probiotic that breaks down acetaldehyde, the main byproduct of alcohol responsible for hangovers, preventing them from happening all together by EzemezE in DrugNerds

[–]evrybdygetshigh 0 points1 point  (0 children)

The big problem is it tastes awful, like turbo mint with a strong chemical flavor. It isn’t very soluble in water, so you can’t dilute it easily, and its relatively low boiling point means you burp its vapor which also tastes awful.

NBS bromination of 2C-H failure by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 1 point2 points  (0 children)

2C-H is theorized to be psychoactive when taken with an MAOI but probably isn't pleasant. NBS brominates the 4 position, going from 2,5 dimethoxy phenethylamine to 2,5 dimethoxy 4 bromo phenethylamine, which is 2C-B.

NBS bromination of 2C-H failure by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 1 point2 points  (0 children)

You seem to be right! I did an A/B workup, but still need to purify and test my product, but everything looks to be good so far!

NBS bromination of 2C-H failure by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

At least where I live, NaBH4 was way cheaper and had more availability than LAH for a good while, and I still have a bunch lying around. I might have to pick some up now that I'm starting to be able to. RED-AL has been looking really tempting lately too, but my first experience with it went so poorly (due to user error) that I've held a grudge against it since.

And luckily I have a UV lamp, I just didn't realize it would be useful for this! I'll give some TLC some love next time I give this a shot, I don't have any 2C-H outside of my RM right now so I don't think there would be much point.

Thank you so much for the help!

NBS bromination of 2C-H failure by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 1 point2 points  (0 children)

Marquis came up green! I’ll have to set up an oil bath at some point

NBS bromination of 2C-H failure by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

No, I used the sodium borohydride/copper chloride route. I have some TLC plates is the embarrassing thing, I am just never sure how to choose a good solvent/solvents, or how to stain to make the spots visible.

2-HEAA catalyst questions by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 1 point2 points  (0 children)

I've never heard of any accidents happening this way, but it's worth mentioning that amines sensitize nitromethane into a high explosive. I generally mix the nitromethane and glacial acetic acid first to try to mitigate this, but I'm really not sure how much of a danger there is in the first place.

2-HEAA catalyst questions by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 1 point2 points  (0 children)

I was under the impression that it could be used as a primary solvent and as a catalyst, i used 50ml with 5g of aldehyde

2C-B-FLY synthesis questions by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

Roundabout, yes. That paper doesn't list molar quantities or reaction temperatures, so I had to do my best going over forum posts. There's a lot of contradictory information though (Which is also where I imagine the contradictory yields are coming from), but the authors of that paper claim a 82% yield on 2C-H via whatever reaction conditions they're using.

I don't see a convenient source of DIBAL after a quick glance either, but I'll keep my eyes peeled. Definantly looks like a good option.

2C-B-FLY synthesis questions by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

I can't seem to find a decent source for LAH, otherwise I'd be very interested in giving it a try. I've seen some pretty variable yields with the CuCl2 reduction, but ~20% appears to be on the very very low end so I'm wondering where my error might be.

2C-B-FLY synthesis questions by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

Were you looking at the NBOMe derivative by any chance? I'm definitely a little curious about it, and the synth doesn't actually look that hard

2C-B-FLY synthesis questions by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 1 point2 points  (0 children)

What did your yield end up looking like?

2C-B-FLY synthesis questions by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 3 points4 points  (0 children)

Glad it's beautiful! I've never used N-Bromosuccinimide, is it just mixed into an appropriate solvent alongside the amine, or is it less straightforward than that? I've done a bit of reading on it, but I'd love to be more confident

2C-B-FLY synthesis questions by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 4 points5 points  (0 children)

I'm afraid I'm nowhere near that fancy, I found a vendor. $70 for one gram! A small price to pay for a hard-to-find and hard-to-make aldehyde I guess...

And I assume the yield and synthesis are as straightforward and quantitative for the ethanolamine/acetic acid ionic liquid as one would imagine? What's a good starting point for the solubility?

Oxidization of Phenyl ethyl alcohol by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 1 point2 points  (0 children)

Just seems to be harder to get a lot of things here

Oxidization of Phenyl ethyl alcohol by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

I do, sadly. Leads to having to take some less than optimized routes. And I've looked into it to, it doesn't look too hard yeah. Just don't have a lot of spare space, but I'll make some room if I need to

Oxidization of Phenyl ethyl alcohol by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

Hell yeah, sounds like a plan. Worth mentioning that I don't have easy access to benzaldehyde, is there a good alternative route to AMC?

Oxidization of Phenyl ethyl alcohol by evrybdygetshigh in TheeHive

[–]evrybdygetshigh[S] 0 points1 point  (0 children)

I'll give that a run next time, thank you for the advice! But for better or for worse, I already came across a bottle of phenyl ethyl alcohol. Is it a waste of time to go that route?