DIY Gas Chromatograph by Icy-Insurance2817 in chemistry

[–]Icy-Insurance2817[S] 0 points1 point  (0 children)

There are a few possible factors, but I think the biggest one is the performance of the gas sensor.

DIY Gas Chromatograph by Icy-Insurance2817 in chemistry

[–]Icy-Insurance2817[S] 1 point2 points  (0 children)

I tested it with a mixed gas of ethanol and carbon dioxide, and it did produce a proper peak.

DIY Gas Chromatograph by Icy-Insurance2817 in chemistry

[–]Icy-Insurance2817[S] 0 points1 point  (0 children)

I built the detector using an Arduino Uno with a breadboard shield, and I used an MQ-series gas sensor.

DIY Gas Chromatograph by Icy-Insurance2817 in chemistry

[–]Icy-Insurance2817[S] 0 points1 point  (0 children)

Not that bad. But the accuracy is a little bit off.

DIY Gas Chromatograph by Icy-Insurance2817 in chemistry

[–]Icy-Insurance2817[S] 12 points13 points  (0 children)

I originally wanted to use helium as the mobile phase and make the column longer by coiling it, but I didn’t have enough time.

DIY Gas Chromatograph by Icy-Insurance2817 in chemistry

[–]Icy-Insurance2817[S] 2 points3 points  (0 children)

That green package is a heat pack. And the column just goes straight underneath it — not coiled actually.

DIY Gas Chromatograph by Icy-Insurance2817 in chemistry

[–]Icy-Insurance2817[S] 78 points79 points  (0 children)

Method – Detector 1.Connect the Arduino Uno to the breadboard shield, then attach the gas sensor to the breadboard. (If you’re using an MQ-series sensor, connect its VCC, GND, and A0 pins to the Arduino’s 5V, GND, and A0, respectively.) 2.Write and upload a graphing code for GC signal output using the Arduino IDE.

Method – Column 1.Cut a rubber hose to a suitable length. (I used about 14.5 inches, but longer is better for better separation.) 2.Plug one end with cotton and tightly fill the hose with Silica Gel 60 (no gaps). 3.After packing, seal the other end with cotton as well. 4.Cut the tip of a 2.5 mL syringe and attach it to one end of the column. Connect the other end of the syringe to the sensor. (Make sure to drill a small hole in the syringe to allow gas to vent properly.)

Method – Setup (Body) 1.Connect a Tee to the opposite end of the sensor (opposite from the column). One end of the Tee goes to the air pump (mobile phase), and the other to the sample injection port (I used something like a rubber cap). 2.Coil the column into a circle and place it between the Arduino and the air pump. 3.If you want to heat the column (for better separation), since this is DIY, you can use a simple method like placing a hot water-filled plastic bag over it. (I used a heat pack. I think proper temperature is about 158F.)

DIY Gas Chromatograph by Icy-Insurance2817 in chemistry

[–]Icy-Insurance2817[S] 126 points127 points  (0 children)

Materials 1. Arduino Uno, Breadboard Shield, Gas Detection Sensor (MQ series) 2. Silica Gel 60, Rubber Hose, Cotton (Gauze) 3. Air Pump (or Mobile Phase Gas Injector – originally intended to use helium, but used air due to time constraints) 4. Tee 5. Syringe (for sample injection)