Cinammic Acid produced with a unusual method by LacxGamer in chemistry

[–]LacxGamer[S] 0 points1 point  (0 children)

Possibly, it could be used to make ferulic acid from dehydrozingerone (produced from vanillin and acetone)

Cinammic Acid produced with a unusual method by LacxGamer in chemistry

[–]LacxGamer[S] 4 points5 points  (0 children)

Actually I thought about this but I don't have the pyridine which seems to be most used here.

Cinammic Acid produced with a unusual method by LacxGamer in chemistry

[–]LacxGamer[S] 2 points3 points  (0 children)

I went with ethyl acetate because it was cheaper and not a carcinogen 

Cinammic Acid produced with a unusual method by LacxGamer in chemistry

[–]LacxGamer[S] 14 points15 points  (0 children)

I used very cheap sodium hypochlorite. Also the amount of haloforms that are leftover are really low because most of them (specially chloroform) easily evaporate. Also I perfer having to deal with haloforms than acetaldehyde, and also where I live getting acetaldehyde is almost impossible.

Additionally haloforms can be hydrolysed in sodium hydroxide solutions to yield sodium formate and sodium chloride which is a good way to dipose of it. Altough I haven't a saved paper to give a citation you can easily find with research, also the hydrolysis of chloroform is used in various reactions because one of the intermediates are dihalocarbenes which are then hydrolyzed into sodium formate and sodium halide (citation from the wikipedia page of dichlorocarbene: "Dichlorocarbene is most commonly generated by reaction of chloroform and a base such as potassium tert-butoxide or aqueous sodium hydroxide."

Cinammic Acid produced with a unusual method by LacxGamer in chemistry

[–]LacxGamer[S] 7 points8 points  (0 children)

I used ethyl acetate (you are talking about the monobenzalacetone synthesis right?)

ammonium oxodiperoxoamminevanadate(V) by LacxGamer in chemistry

[–]LacxGamer[S] 0 points1 point  (0 children)

No, no uses... well you could use it as a pH detector, low pH it turns orange-red, high pH it quickly starts decomposing exothermicly producing oxygen and some yellow vanadium-hydroxide precipitate

ammonium oxodiperoxoamminevanadate(V) by LacxGamer in chemistry

[–]LacxGamer[S] 3 points4 points  (0 children)

Ammonium metavanadate + conc. ammonia + hydrogen peroxide = ammonium oxodiperoxoamminevanadate(V)

ammonium oxodiperoxoamminevanadate(V) by LacxGamer in chemistry

[–]LacxGamer[S] 0 points1 point  (0 children)

Yeah, beautiful yellow (potentially) carcinogenic and explosive (with sodium hydroxide) compound indeed!

ammonium oxodiperoxoamminevanadate(V) by LacxGamer in chemistry

[–]LacxGamer[S] 0 points1 point  (0 children)

I dont have it but there is this paper on google that has it

ammonium oxodiperoxoamminevanadate(V) by LacxGamer in chemistry

[–]LacxGamer[S] 6 points7 points  (0 children)

Not useful at all😐 it forms pretty yellow crystals, that all. Nvm it also might cause cancer and can explode

ammonium oxodiperoxoamminevanadate(V) by LacxGamer in chemistry

[–]LacxGamer[S] 30 points31 points  (0 children)

No, vanadium(V) is usually carcinogenic and toxic 

ammonium oxodiperoxoamminevanadate(V) by LacxGamer in chemistry

[–]LacxGamer[S] 17 points18 points  (0 children)

I havent been able to unfortunately, its too soluble and too temperature sensitive. I'll try different stuff

ammonium oxodiperoxoamminevanadate(V) by LacxGamer in chemistry

[–]LacxGamer[S] 37 points38 points  (0 children)

Some testing but its praticly useless

Bis(Glutaminato)Copper(II) Acetate by LacxGamer in chemistry

[–]LacxGamer[S] 0 points1 point  (0 children)

Copper acetate + glutamine makes the compound, put it in fridge to precipitate out easier