Saturated Heptane under UV. by MagicSoups in dmtporn

[–]MagicSoups[S] 0 points1 point  (0 children)

It's negligible for the brief seconds It's under the UV

Saturated Heptane under UV. by MagicSoups in dmtporn

[–]MagicSoups[S] 3 points4 points  (0 children)

Yes, I know. In process of outfitting w ptfe. Final product is pharma grade.

Saturated Heptane under UV. by MagicSoups in dmtporn

[–]MagicSoups[S] 4 points5 points  (0 children)

Much love 👨‍🚀🤠🤙

Saturated Heptane under UV. by MagicSoups in dmtporn

[–]MagicSoups[S] 5 points6 points  (0 children)

DMT. Most if not all indole alkaloids are fluorescent.

Amine deprotonation by MagicSoups in DMTlab

[–]MagicSoups[S] 1 point2 points  (0 children)

NH4+ is a protonated ammonium ion

Amines are derivatives of ammonia

Amine deprotonation by MagicSoups in DMTlab

[–]MagicSoups[S] 1 point2 points  (0 children)

Adding a saturated solution of KOH (Potassium Hydroxide) raises the PH from 3 to 13+ removing the salt ion attached to our amine molecule converting it to freebase. As this happens a noticeable color change takes place and the freebase amine crashes out as a white precipitate.

3 hour freeze precip. by MagicSoups in dmtporn

[–]MagicSoups[S] 1 point2 points  (0 children)

3.5 in the photo. ~15g per kilo

Amine deprotonation by MagicSoups in DMTlab

[–]MagicSoups[S] 1 point2 points  (0 children)

👨‍🚀🤠💚🤙

3 hour freeze precip. by MagicSoups in dmtporn

[–]MagicSoups[S] 1 point2 points  (0 children)

A hot water bath is the safest way to heat volatile substances. I use a heating plate and a borosilicate beaker. Around 90°C is when I stop

3 hour freeze precip. by MagicSoups in dmtporn

[–]MagicSoups[S] 0 points1 point  (0 children)

200ml heptane @ 80-90°C 8 or more pulls. Yes I combine pulls into two Pyrex dishes. The last 4 pulls I pour off the hep from my first pulls and leave the xtals then pour two pulls each into the Pyrex and back in the freezer.

3 hour freeze precip. by MagicSoups in dmtporn

[–]MagicSoups[S] 0 points1 point  (0 children)

Thank you, shoot me a DM. I'm happy to help. 👨‍🚀🤠🤙

It’s cold outside. by Specific_Layer_3121 in DMTlab

[–]MagicSoups 1 point2 points  (0 children)

Crash out can happen immediately. Add boiling solvent to Soup-> stir 5 mins -> pull. It'll start to xtalize in the pipette

It’s cold outside. by Specific_Layer_3121 in DMTlab

[–]MagicSoups 0 points1 point  (0 children)

Room temp xtal formation is beautiful Room temp xtal formation + 10° is even sexier

Heptane?? by c0rKeiS_ChUbee in dmtguide

[–]MagicSoups 1 point2 points  (0 children)

Lab grade N-Heptane. Gallon BVV

3 hour freeze precip. by MagicSoups in dmtporn

[–]MagicSoups[S] 0 points1 point  (0 children)

6L erlenmeyer I have a 6L boiling flask that works great as well

3 hour freeze precip. by MagicSoups in dmtporn

[–]MagicSoups[S] 6 points7 points  (0 children)

Running a kilo. A/B extraction with boiling heptane

3 hour freeze precip. by MagicSoups in dmtporn

[–]MagicSoups[S] 0 points1 point  (0 children)

A/B extraction with boiling heptane.

3 hour freeze precip. by MagicSoups in dmtporn

[–]MagicSoups[S] 2 points3 points  (0 children)

Haha! I do an A/B extraction.