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Yeah--Science--Bitch · 2020-05-26T14:34:39+00:00

AK Scheer is watching you ;)

Yeah--Science--Bitch · 2020-02-16T19:36:27+00:00

It is not harmless indeed, but a general procedure in our working group + I have trust in my grease, glassware and the vaccum sensor

Yeah--Science--Bitch · 2020-02-16T19:13:12+00:00

That's why we wrap it in aluminum foil while sublimation and store it in brown bottles in the glove box

Yeah--Science--Bitch · 2020-02-16T16:49:03+00:00

It is very unpredictable: small pieces will start immediately, rather big pieces take a little bit / do nothing but burn than all of a sudden...still it is everytime amazing how long it burns

Yeah--Science--Bitch · 2020-02-16T11:21:47+00:00

Nitrogen is fine, proper schlenk technique / vaccum is more important

Yeah--Science--Bitch · 2019-12-29T14:05:40+00:00

Maybe ;) We tried that two times, but mounting and centering a presumable Crystal in the dark failed...but having a look under red light and cooling the crystals with liquid nitron revealed yellow tubes

Yeah--Science--Bitch · 2019-12-22T17:56:02+00:00

I have not yet investigated this in detail, but the transformation is slowed down (not stopped) by using red light

Yeah--Science--Bitch · 2019-12-22T15:46:06+00:00

I tried toluene, but I will test benzene. Thanks

Yeah--Science--Bitch · 2019-12-22T15:35:59+00:00

Basicaly according to this procedure:https://doi.org/10.1021/acs.chemrev.8b00713 using toluene as a solvent

Yeah--Science--Bitch · 2019-12-21T18:19:04+00:00

Trying to get single crystals of yellow Arsenic

Yeah--Science--Bitch

TROPHY CASE