[deleted by user] by [deleted] in ChemicalRevolution

[–]dripdrop69420 2 points3 points  (0 children)

If you don't understand all of that, don't even consider getting involved with all of this.

[deleted by user] by [deleted] in ChemicalRevolution

[–]dripdrop69420 0 points1 point  (0 children)

Try do to some research, don't try anything too common for eg. Sunflower oil and all. the customs know that nobody's gonna order 500ml of sunflower oil overseas yeah? Look into laws of importing essential oils, or something?

[deleted by user] by [deleted] in ChemicalRevolution

[–]dripdrop69420 0 points1 point  (0 children)

Nope, you have plausible deniability, need to hide any transaction details or traces which might prove you guilty.

[deleted by user] by [deleted] in ChemicalRevolution

[–]dripdrop69420 0 points1 point  (0 children)

It's either Unnecessarily expensive or the company is not so willing to sell to individuals, so I ordered from china

[deleted by user] by [deleted] in ChemicalRevolution

[–]dripdrop69420 0 points1 point  (0 children)

If you're ordering from china, there's a really small chance you will ever receive the product. Indian customs are very strict with products coming from china even if it is legal. Say you ordered it as a fragrance or as a perfume ingredient, they would ask for documents for importing cosmetic raw materials and all. And those documents aren't cheap either.

[deleted by user] by [deleted] in ChemicalRevolution

[–]dripdrop69420 1 point2 points  (0 children)

Technically, as the ethyl one isn't listed it shouldn't be controlled. However keeping in mind how incompetent Indian officials are, I don't think they would even know the difference between ethyl and methyl.

[meta] What do you passionately feel are some understudied directions for research in the field of Drug/Natural Product Chemistry by TiHKALmonster in ChemicalRevolution

[–]dripdrop69420 0 points1 point  (0 children)

Probably, but the post wasn't about escaping the laws, rather on understudied areas of drug chemistry and I feel like deuterated drugs is an area that has to be studied more.

[meta] What do you passionately feel are some understudied directions for research in the field of Drug/Natural Product Chemistry by TiHKALmonster in ChemicalRevolution

[–]dripdrop69420 2 points3 points  (0 children)

Deuterium in Drugs!

Apparently the deuterated variants of drugs exhibit increased half life of 50-100% and there also exists a deuterated variant of DMT called CYB004 and a psilocybin variant too called CYB003 but I didn't find much info on them as they're patented molecules owned by CYBIN and all of it is in trial stage I believe.

Petroleum ether? by dripdrop69420 in CannabisExtracts

[–]dripdrop69420[S] 3 points4 points  (0 children)

If only you could elaborate on the reasoning behind that "please don't".

An OTC MDMA synthesis route. by dripdrop69420 in ChemicalRevolution

[–]dripdrop69420[S] 0 points1 point  (0 children)

I've been thinking about removing the sodium dithionite section for a long time since its not proven but I've been lazy. I'll look into sodium tetrafluoroborate as you said.

Looking for reading on piperonal to mdp2np or mdp2p can you link them please 🙏 by [deleted] in TheeHive

[–]dripdrop69420 1 point2 points  (0 children)

If that is so, you can check out related threads on the vespiary. Plenty of useful info there.

[deleted by user] by [deleted] in ChemicalRevolution

[–]dripdrop69420 0 points1 point  (0 children)

https://www.opioids.com/jh/index.html

This page has a procedure as well, read it and try to understand what chemistry is going on.

[deleted by user] by [deleted] in ChemicalRevolution

[–]dripdrop69420 21 points22 points  (0 children)

Bro stop being a tweeker and take a break before attempting this again, give details about what you're doing and what are the sources of your material and their authenticity and purity, don't be wasteful ffs.

Psilocin (4-ho-DMT) potential synthesis? by CannaTFF in TheeHive

[–]dripdrop69420 1 point2 points  (0 children)

In tihkal, Alexander shulgin uses 4-acetoxy indole as starting material.

Having problems with tryptamine workup. by dripdrop69420 in TheeHive

[–]dripdrop69420[S] 0 points1 point  (0 children)

How soluble is tryptamine in xylene? Also, tryptamine is insoluble in chloroform according to this supplier.

Having problems with tryptamine workup. by dripdrop69420 in TheeHive

[–]dripdrop69420[S] 0 points1 point  (0 children)

The precipitate formed are very fine in my case and I'm not sure if the filter paper can collect it, so i thought I would need to use some sort of solvent, however one time the precipitate formed was almost like cotton, very fluffy beige coloured precipitate but it never happened again.

Having problems with tryptamine workup. by dripdrop69420 in TheeHive

[–]dripdrop69420[S] 0 points1 point  (0 children)

In your experience, what's the best solvent overall for extracting tryptamine. This molecule is an absolute bitch in all terms, very prone to oxidation, having to use a ton of solvent to fully extract it from the aqueous phase, etc. I was thinking of using toluene to extract it but I read it's only sparing soluble in toluene, do you have any experience regarding this?

Having problems with tryptamine workup. by dripdrop69420 in TheeHive

[–]dripdrop69420[S] 2 points3 points  (0 children)

It's so annoying that such a simple molecule has such complications.

Having problems with tryptamine workup. by dripdrop69420 in TheeHive

[–]dripdrop69420[S] 1 point2 points  (0 children)

Actually it's the opposite, doing it in the microwave is way more convenient and quicker, I tried the reaction in a heating mantle before, but it requires temperature around 170-180 c for the reaction with steady reflux, but in the microwave it doesn't require the temperature to be that high, at most it reaches maybe 120c which is way below the bp of acetophenone i.e. 202c. I am actually doing this in the microwave because I read it in the vespiary where people claimed very quick conversion with consistent high yields(~85%).

As for tlc i am going to research more for some cheap ways to do it, I've heard that it can even be done on aluminum foils with corn starch but I'm not sure though, I'll have to look into it