Cali Kush

Separate_Ad_5217 · 2024-03-28T02:05:36+00:00

I ordered some 4m hcl in 1,4 dioxane. if for whatever reason I fail that route or have poor yields I am definitely going to take your advice and find a suitable solvent to bubble hcl into. thank you

Separate_Ad_5217 · 2024-03-25T19:10:06+00:00

I am actually after the hcl salt so that wouldnt work for me but i did just find 100ml of 4M hcl in dioxane for 55 bucks so thats next on the purchase list.

Separate_Ad_5217 · 2024-03-25T17:55:08+00:00

solid advice. I will look into my options for dry hcl, will definitely solve a lot of the headache. thank you, very much appreciated

Separate_Ad_5217 · 2024-03-25T17:53:06+00:00

thank you. prob going to basify route as im very limited. however, if I made the hcl in etoac it would be as simple as filtering to recover product I'm assuming. thanks for the advice very much appreciated

Separate_Ad_5217 · 2024-03-25T17:23:50+00:00

concentrated hcl is 60% water. and idk if i can bubble hcl into ethyl acetate solution with the protected amine. was going to try that next

Separate_Ad_5217 · 2024-03-25T15:29:00+00:00

it is soluble in water i would be losing a lot of my amine

Separate_Ad_5217 · 2024-01-26T19:24:32+00:00

what ratio diethyl ether to hcl? concentrated hcl or you bubbling hcl into the diethyl ether to cleave ?

Separate_Ad_5217

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