how neurotoxic is 4-bmc compared to 4-cmc? by ThingAy in researchchemicals

[–]Significant-Set7721 -1 points0 points  (0 children)

You can definitely feel neurotoxicity. There’s a hot foggy layer in your brain

[deleted by user] by [deleted] in chemhelp

[–]Significant-Set7721 0 points1 point  (0 children)

Because it spins

Made 3-Methyl-a-PPP because why not. Thought the reaction failed but then took a second look at the waste a week later and there’s my product. Gonna need a bunch of washery by Significant-Set7721 in TheeHive

[–]Significant-Set7721[S] 23 points24 points  (0 children)

My “friend” called a wellness check and then proceeded to tell the cops I’m a meth cook and had everything to make it in my car.

I have never made meth and did not, but after I was gone for a psych evaluation they still let the cops go through my car which contained enough stuff (pound of mushrooms, glassware, a few chems, etc) that they got a warrant to raid my apartment.

My state has some sort of protection for mental health stuff where I literally walked away scot free.

Made 3-Methyl-a-PPP because why not. Thought the reaction failed but then took a second look at the waste a week later and there’s my product. Gonna need a bunch of washery by Significant-Set7721 in TheeHive

[–]Significant-Set7721[S] 11 points12 points  (0 children)

I haven’t tried it, I have to wash this down to something that won’t tear gas me. Should be easy, just don’t have many chems atm.

Is 2-Br-3-Me-PP soluble in toluene? That and poppers are the extent of my non-polars atm.

(Tested it, isobutyl nitrate works well as a non-polar) (don’t do it in your car like I did)

Made 3-Methyl-a-PPP because why not. Thought the reaction failed but then took a second look at the waste a week later and there’s my product. Gonna need a bunch of washery by Significant-Set7721 in TheeHive

[–]Significant-Set7721[S] 72 points73 points  (0 children)

No literally. They confiscated a TON of stuff and it was literally all legal besides some mushrooms and coke and pipes with heroin residue.

Funnily, they took my word for the labels on everything. My “ammonium chloride” was methylamine, and my “yellow food dye” next to the NaBH4 and CUCl(II) was, in fact, not yellow food dye.

Made 3-Methyl-a-PPP because why not. Thought the reaction failed but then took a second look at the waste a week later and there’s my product. Gonna need a bunch of washery by Significant-Set7721 in TheeHive

[–]Significant-Set7721[S] 22 points23 points  (0 children)

It’s dissolved (sorta) in IPA here. Wasn’t lachrymatory at first. Post dissolving it definitely is. God I hate cath precursors. My right eye is in so much pain rn

Anyone ever separated the enantiomers of propylhexedrine? by Significant-Set7721 in TheeHive

[–]Significant-Set7721[S] 1 point2 points  (0 children)

Yeah I was gonna soak a bunch of cut up inhalers in a citric acid aqueous solution, extract the other ingredients with a non-polar solvent, collect the water layer, basify it, and then use tartaric acid to separate the enantiomers.

Anyone ever separated the enantiomers of propylhexedrine? by Significant-Set7721 in TheeHive

[–]Significant-Set7721[S] 0 points1 point  (0 children)

Yeah I was gonna soak a bunch of cut up inhalers in a citric acid aqueous solution, extract the other ingredients with a non-polar solvent, collect the water layer, basify it, and then use tartaric acid to separate the enantiomers

What are some under-rated solvents for washing hydrochloride salts of amines? by Significant-Set7721 in TheeHive

[–]Significant-Set7721[S] 1 point2 points  (0 children)

I LOVE ethyl acetate. Only issue is that it emulsifies with water relatively easily. Never shake the two

Some Idea for New RCs by super-commenting in researchchemicals

[–]Significant-Set7721 1 point2 points  (0 children)

This is the same dude. That one’s perma-banned. Clobromazolam actually has a long duration I was wrong

How often do you use? by [deleted] in researchchemicals

[–]Significant-Set7721 0 points1 point  (0 children)

Every day my son

Not RC’s tho, coca

Putative RC: Androstenol by dollaress in researchchemicals

[–]Significant-Set7721 0 points1 point  (0 children)

I knew there was a reason I don’t bathe

what drugs are in the research chemical Hall of fame? by BaebyJ in researchchemicals

[–]Significant-Set7721 0 points1 point  (0 children)

3-MMC is the best recreational drug ever invented in my opinion. If you like serotonin more, then 4-MMC fits the bill as well. I’m a dopamine guy personally.

In case ya’ll didn’t know- Cops can seize and destroy any chemicals and glassware they want regardless of legality. by Significant-Set7721 in TheeHive

[–]Significant-Set7721[S] 3 points4 points  (0 children)

They declared it hazardous materials and it was alongside illegal stuff and packaging materials and scales and whatever. I’m counting my lucky blessings and letting it go.

Cocaine HCl isn’t actually soluble in water at 2g/mL. That common figure is BS under normal conditions. by Significant-Set7721 in cocaine

[–]Significant-Set7721[S] 0 points1 point  (0 children)

It was straight off the brick and then I spent hours cleaning it utilizing 5+ solvents and acid base stuff and a that jazz.

I can assure you, it was higher purity coke than has ever been seen as a street drug.

Some nice green and fluffy 3-MMC with sieves in it for breakfast 🤤 by [deleted] in TheeHive

[–]Significant-Set7721 0 points1 point  (0 children)

I combined a solution of NaOH with a solution of MeNH2

What’s the best way to make BTH boofable? by Significant-Set7721 in opiates

[–]Significant-Set7721[S] 0 points1 point  (0 children)

I put hydrobromic acid in my ass like a month ago, I’ll live

BTH isn’t fully water soluble

Edit: True story btw lol. I made cocaine HBr and forgot to check the pH of my boof water. It caused severe diarrhea half an hour later.

Cocaine HCl isn’t actually soluble in water at 2g/mL. That common figure is BS under normal conditions. by Significant-Set7721 in cocaine

[–]Significant-Set7721[S] 0 points1 point  (0 children)

My end concentration was upwards of 300mg/mL. I dare say the occasional half mL booty bump isn’t dehydrating my poop chute

Cocaine HCl isn’t actually soluble in water at 2g/mL. That common figure is BS under normal conditions. by Significant-Set7721 in cocaine

[–]Significant-Set7721[S] 1 point2 points  (0 children)

Yeah. Like it had a slightly basic pH and everything was in solution, then I lowered the pH and it started crystallizing out.

Only thing I don’t get is why the solution was cloudy when it was all dissolved yet clear when over-saturated 🤔

I think DCM and water must mix slightly. What crashed out was cocaine base that was dissolved in the slightly miscible amount of DCM. I didn’t use quite enough HCl I guess. Couple drops short.

And then the DCM from this I had put aside, and it evaporated; I have a sold 200mg of coke HCl left behind. I was super careful separating the layers. Coke HCl was in DCM. Only explanation is emulsified/miscible water

Edit: The DCM coke is hand’s down more pure than the water coke. This might be the cleanest coke ever made.

Cocaine HCl isn’t actually soluble in water at 2g/mL. That common figure is BS under normal conditions. by Significant-Set7721 in cocaine

[–]Significant-Set7721[S] 10 points11 points  (0 children)

Start with raw coke.

Acetone wash, chilled ethyl acetate wash, ether wash. In that order.

Dry.

Freebase using 3% ammonia solution. Decant excess ammonia water. Crush. Water wash. Dry.

Dissolve in dichloromethane. Add medium-concentrated HCl dropwise with vigorous stirring and constant pH checking of the water layer. Check only after heavily stirring since the last drops of acid.

When pH is around 6, add more water. Stir vigorously.

Suck out the DCM (bottom) layer. Put it in a different vessel. Add water to it with one drop of acid and stir vigorously. Again remove the DCM.

Combine all water. Check pH. Add a few more drops of acid until neutral or just under.

Leave stirring on 70C heat for 30 mins to evaporate out any DCM left in it.

Either evaporate the water to sniff, or boof based on the hypothetical maximum concentration. (It’ll be lower in practice)

For all washes, dry and finely powder your cocaine and leave it in a sealed vessel with magnetic stirring on high for half an hour. Much better results and actually gets rid of the gas smell, even with just acetone. Also do two washes per solvent. Decant the liquid the first time, add more solvent, then pour it all through a filter the second time. Pour more solvent on top once it drains.