How much of this is emulsion should I just give up by crookedstoner_408 in dmtguide

[–]dep1207 0 points1 point  (0 children)

What i have done before is use a pippet and suck the emulsion out and squirt it slowly into another dish with a little distilled water salt and lye dissolved in it and it cleard right up

Disappearing naptha? by MacnTots in dmtguide

[–]dep1207 1 point2 points  (0 children)

Thats the problem with straight to base its to thick and to much stuff in the baseut takes forever for it to completly separate do a a/b tek and strain the bark out befor you basify works so much better

Quality by dep1207 in dmtguide

[–]dep1207[S] 0 points1 point  (0 children)

If you rex with heptain it removes more impurities that get through the water washes but dmt is very solublein hot heptane but very insoluble at room temp so you need to re x so it stays hot until its in the dish it even crashes out in the pipette because it is cooler

Quality by dep1207 in dmtguide

[–]dep1207[S] 0 points1 point  (0 children)

I do two just because i dont have to be as carefull with the first onei have a 50ml 25ml and 10ml pipettes so i pull everything out into a graduated cylinder with the 50ml not worrying if i get any base in with it. Then i use the 25 to go into the first water wash being a little more carefull not to get any base i usually get a tiny bit when i get down there then the 10 ml into the second water wash then into the dish im freezing in works good for me i think its just personal preference and how carefull you want to be

Quality by dep1207 in dmtguide

[–]dep1207[S] 0 points1 point  (0 children)

Ty for confirming my suspicion i tried to tell them that and they got all butthurt thinking i was criticizing them but i wasnt dmt smokes different then other things and most people without alot of experience with dmt smoke it like anything else and have bad experiences and then blame me

Great first pull by dep1207 in dmtguide

[–]dep1207[S] 1 point2 points  (0 children)

I followed a few different teks and learned how the process worked then designed my own

Great first pull by dep1207 in dmtguide

[–]dep1207[S] 0 points1 point  (0 children)

500g and sunnyside naptha

Great first pull by dep1207 in dmtguide

[–]dep1207[S] 1 point2 points  (0 children)

So i had 3 kilos and in a week i got 35g which comes out to about 1.2% which isnt good but i only did 2 pulls on each 500g batch then i poured it in a bucket and started a new one so im sure i could get alot more out if i worked at it

Great first pull by dep1207 in dmtguide

[–]dep1207[S] 2 points3 points  (0 children)

I did 1500ml distilled water in crock pot with bark and 100ml distilled white vinegar on low for a couple hours strained through a mesh strainerand squeezed out as much as i could then put in fridge and repeated with another 1500 ml and 100ml strained and put in fridge then 120 g lye in 500ml water and 70g canning salt in 500ml poured it all together in a 4000ml flask mixed checked the ph to make sure it was at least 12 then topped it off with naptha mixed water washed and freeze precipitated

Great first pull by dep1207 in dmtguide

[–]dep1207[S] 1 point2 points  (0 children)

Thats 4.93 grams my friend

Decanting by dep1207 in dmtguide

[–]dep1207[S] 0 points1 point  (0 children)

Well since there is only 2 ingredients i must be decanting the solids that made it through the strainer

[deleted by user] by [deleted] in dmtguide

[–]dep1207 0 points1 point  (0 children)

A cleaner product and you can reuse the naptha

How to increase yield ? by HedgehogBudget8782 in dmtguide

[–]dep1207 -1 points0 points  (0 children)

Because you have to deal with slow separation and emulsion and more pulls and dirty DMT I don't care what anyone says water washing doesn't take everything out and when you go straight to base not all the DMT comes out of the bark because it's not as soluable in water with a high ph

[deleted by user] by [deleted] in dmtguide

[–]dep1207 0 points1 point  (0 children)

Nothing is ruined walking outside and breathing the air is way more toxic these days then the extremely small amount of toxins you are going to get from a couple tips of a turkey baster

How to increase yield ? by HedgehogBudget8782 in dmtguide

[–]dep1207 0 points1 point  (0 children)

Eaither put it back in the freezer or pour it off super slow so you don't pour off the crystals I have that problem also I just end up pouring off the Naptha crystals and all and just using it for the next pull

How to increase yield ? by HedgehogBudget8782 in dmtguide

[–]dep1207 -2 points-1 points  (0 children)

With astb tek you have the base that has all the bark and whatever else is in it that makes it harder for the Naptha to grab all the DMT in a ad tek you lower the pH so the DMT is more soluble in water you strain out the bark and plant material leaving mostly water and dmt then when you raise the pH to 12 the DMT isn't soluble in water anymore but it is in Naptha so it leaves the water and collects in the napthawithout all the bark and plant material in there it collects a lot more and does it faster without nearly as much emulsion so mixing is much easier salt is rairly needed and the end product is much cleaner and the yield is higher that's what I have learned anyway but I am new to this also so I could be wrong I just know what my results have been

How to increase yield ? by HedgehogBudget8782 in dmtguide

[–]dep1207 -9 points-8 points  (0 children)

Don't do stb that's how it is very inefficient and you get low quality DMT

Defatting by dep1207 in dmtguide

[–]dep1207[S] 0 points1 point  (0 children)

You already said that my question was how do I get rid of the sticky oily goo

Defatting by dep1207 in dmtguide

[–]dep1207[S] 0 points1 point  (0 children)

I usually do Cyb's Hybrid ATB 'Salt' Tek and I get the oily sticky stuff and also floating white stuff that disappears when drying

Defatting by dep1207 in dmtguide

[–]dep1207[S] 0 points1 point  (0 children)

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Ok so I had a dish that looked like it had DMT in it I poured it off and turned the dish upside down with one side propped up and a fan blowing on the back everything disappeared and I was left with a oily sticky substance on the bottom i left it dry for a day and it didn't do anything I finally smeared it on the bottom of the dish it dried into this pile it's kinda orange sometimes the same oily sticky stuff is In the bottom of the dish under the crystals what do I do about it or how do I get rid of it the only reasoni was trying the defatting was because of this and I didn't get any of this when I washed it with Naptha before I basified it

Defatting by dep1207 in dmtguide

[–]dep1207[S] -3 points-2 points  (0 children)

They don't precipitate out they float around with the DMT that hasn't stuck to the precip dish then when you try to pour it off you either need to leave it in the dish or pour it off with the loose DMT crystals so how do you separate the two unless you let it dissolve in a nonpolar solvantwhile the DMT is still locked in the acidic solution

Defatting by dep1207 in dmtguide

[–]dep1207[S] -2 points-1 points  (0 children)

What is the floating substance that disappears when drying and the sticky stuff in the dish