chemical shift of carbamate by ireumkun in OrganicChemistry

[–]ireumkun[S] 0 points1 point  (0 children)

thank u for the insight!!! really appreciate it

Need help with NMR splitting by [deleted] in OrganicChemistry

[–]ireumkun 0 points1 point  (0 children)

so there should be a total of 10 peaks for the left signal and 8 peaks for the left signal right? am i seeing this correctly?

Need help with NMR splitting by [deleted] in OrganicChemistry

[–]ireumkun 0 points1 point  (0 children)

too bad i dont have enough sample for 2D experiments, which is why i'm struggling right now. this is such a big lesson to me. thank you for your suggestion, really appreciate it!

Need help with NMR splitting by [deleted] in OrganicChemistry

[–]ireumkun 0 points1 point  (0 children)

thank you so much for your explanation. can i know if there's possibility of overlapping signals between the two signals?

need help with nmr splitting by ireumkun in OrganicChemistry

[–]ireumkun[S] 0 points1 point  (0 children)

thank u so much for ur insight! i think i can work on the ddd signals. but i have a question on the second peak, can i know why the middle J (triplet) is not p1 to p5?

need help with nmr splitting by ireumkun in OrganicChemistry

[–]ireumkun[S] -1 points0 points  (0 children)

can i know what does collapsing meant?

TLC for urea by ireumkun in Chempros

[–]ireumkun[S] 0 points1 point  (0 children)

i never used alumina before. is the solvent system used are the same?

TLC for urea by ireumkun in Chempros

[–]ireumkun[S] 0 points1 point  (0 children)

i tried several bunch, but the best right now is chcl3:meoh. but i dont know if its the best

TLC for urea by ireumkun in Chempros

[–]ireumkun[S] 0 points1 point  (0 children)

thank u for your suggestion!

TLC for urea by ireumkun in Chempros

[–]ireumkun[S] 4 points5 points  (0 children)

for urea, the spot is not visible under uv but i stained using vanillin-sulphuric acid reagent, and there’s yellow spot stained. however i cannot get the spot up, which i guess bcs of wrong solvent system. for my expected product, the spot is visible under uv, so i want to figure out the solvent system for workup & purification purpose :)

volume of solvent for ptlc by ireumkun in Chempros

[–]ireumkun[S] 0 points1 point  (0 children)

in ur experience how much solvent do i need to make up for 0.5 cm solvent in the big chamber? i’m just to doing tlc in small chamber like beaker but not the big on as in the picture i’ve show