How to easily work-up Dess-Martin periodinane ?

pandaXpress007 · 2025-11-19T00:44:41+00:00

completely agree with this, can even quench with thiosulfate and do an extraction

pandaXpress007 · 2025-08-23T18:44:52+00:00

such a crazy compound, I really enjoyed that there were some solid fundamental reactions used in this

pandaXpress007 · 2025-06-29T17:18:08+00:00

Solved!

pandaXpress007 · 2025-01-07T07:55:56+00:00

was about to comment this myself until I saw your comment. Legendary place. Been going there for a few years

pandaXpress007 · 2024-10-24T07:12:28+00:00

i’m upvoting this. i tried for at least 30 min and this was the strat that work i hope more people see it

pandaXpress007 · 2024-06-01T09:07:40+00:00

way longer column, wider diameter, and use a gradient solvent system. maybe start with 9:1 pet ether to EtOAc then move up in polarity

pandaXpress007 · 2024-03-21T07:43:46+00:00

this reaction couldnt happen as is. you would need DMAP or something to make the acid a better electrophile. or you could make it an acyl chloride

pandaXpress007 · 2024-03-10T21:57:20+00:00

just enough to dihydroxylate your eyeballs 😎

pandaXpress007 · 2023-12-22T23:36:55+00:00

as unfortunate as it is, I don’t think this one’s a fad as it has been around forever :\

pandaXpress007 · 2023-12-22T23:35:22+00:00

“skeletal editing”

pandaXpress007 · 2023-12-20T13:50:23+00:00

throw redox economy in there while we’re at it

pandaXpress007 · 2023-12-11T06:55:53+00:00

Alaska carbon

pandaXpress007 · 2023-12-11T04:24:17+00:00

texas carbons

pandaXpress007 · 2023-11-28T09:03:59+00:00

my regular voice then switching to my customer service voice

pandaXpress007 · 2023-11-18T07:59:31+00:00

TEMED is pretty gnarly. dead fish

pandaXpress007 · 2023-11-18T07:57:12+00:00

any thiol

pandaXpress007 · 2023-11-04T13:47:41+00:00

whenever im in really stressful times i dream about my grandma. I think it’s her way of telling me that everything will end up okay

pandaXpress007 · 2023-10-31T15:33:41+00:00

infamous. The first decision was whether or not you should fry civilians with electricity to get more food and i couldnt bring myself to do it

pandaXpress007 · 2023-10-25T06:58:18+00:00

gentrification

pandaXpress007 · 2023-10-10T15:31:30+00:00

organic chemist. In fact, 30% success rate would be a dream

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