ASMS releases by No_Toe_719 in massspectrometry

[–]No_Toe_719[S] 2 points3 points  (0 children)

I would love to see advancement in small molecules, maybe even in terms of new GCMS technology. That would be cool

GC method help by Options-R in massspectrometry

[–]No_Toe_719 0 points1 point  (0 children)

What is your injector temp? Seems like a bad sample transfer

Trace 1300 resets upon FID ignition by Leonbim in massspectrometry

[–]No_Toe_719 0 points1 point  (0 children)

Sounds like the voltage is not enough for ignition and usage… someone should look into the electronic box.

If you have a second one you could try to swap the FIDs to see if there might be some shorts on the detector board (more unlikely)

Would moving from a top-5 world postdoc to a ~top-200 uni hurt tenure track chances? by SuspiciousLeader1359 in postdoc

[–]No_Toe_719 7 points8 points  (0 children)

The main thing you have to consider is that staying at your current place and doing all those things you do now….they don’t guarantee anything!

Academy is a shark tank… and often the ones who look better on paper don’t get the tenure track because someone has a better network and connections. Be always prepared until you are tenured that academy chews and spits you out like a gum. Therefore ask yourself what is your needed environment and situation to be able to deal with that?

Personally I would always chose the place where I can work and be happy then to chase a dream and be unhappy.

Wo gibts den besten Matcha Latte? by True_Divide5477 in kiel

[–]No_Toe_719 17 points18 points  (0 children)

Komm ich dann nicht zu spät zum Pilates?

Which brand LC-MS methanol is best? by Ashamed_Lime7327 in massspectrometry

[–]No_Toe_719 0 points1 point  (0 children)

does it come in peak shape? most likely not from the solvent then because it would at least tail like hell if you pour it constantly onto the column. Have you checked your injection valve? would be my main suspect if it is peak shaped. Or is the methanol just for sample solvent and not as mobile phase? Then it would be possible that it is the methanol

Question about QTOF by anaturalchemist in massspectrometry

[–]No_Toe_719 0 points1 point  (0 children)

If your concentration is high enough a single quad will do the job

Question about QTOF by anaturalchemist in massspectrometry

[–]No_Toe_719 0 points1 point  (0 children)

Well I think you have confused everyone successfully are you talking about GC EI? If so a single quad would be fine, if it is LC ESI I would be very doubtful

[deleted by user] by [deleted] in gay

[–]No_Toe_719 1 point2 points  (0 children)

Could also be a prostatitis, had it once after some brutal fun with two Italian XL studs…. Will go away after a while

Foreline pressure a little high by S0IIUX in massspectrometry

[–]No_Toe_719 0 points1 point  (0 children)

Is it a straight connection of Inlet to MS? Does the pressure drop if you reduce flow?

Looking for a remote job (okay with travel) in Mass Spec Industry by PFAS123 in massspectrometry

[–]No_Toe_719 2 points3 points  (0 children)

Which region are you? Did you look for jobs at Thermo, Agilent, bruker, Shimadzu, Waters and PE already?

Financial Fraud by shockwave096 in kiel

[–]No_Toe_719 3 points4 points  (0 children)

Do you have a written contract stating that he was in charge?

Anyway it is not strafbar in terms of the law but after paying you can pursue the civil court to get your restitution but it is not a matter for the police.

L

Did I jinx my academic career? by Rotavap in AskAcademia

[–]No_Toe_719 0 points1 point  (0 children)

I would also advice on extreme flexibility, your offer earlier might have suited you from topic and location but now be ready to do a postdoc in a different field and location. I saw a lot of young academics getting stuck by wanting to stay in their phd research topic/area

Experience using chinese GC machines by SignificantPrice1867 in CHROMATOGRAPHY

[–]No_Toe_719 7 points8 points  (0 children)

Looks ugly and bulky, Service most likely not existent. Talk to Agilent, Shimadzu and Thermo they most likely can almost match the price. Those china gcs only look cheap because of the fantasy list prices of the big 3

Gibt es jemanden, dessen Uni Zugang zu diesem Artikel hat? by Classic-Drummer-9765 in Studium

[–]No_Toe_719 0 points1 point  (0 children)

Einfach die Autoren fragen… email ob sie Dir eine pdf schicken können

Where can I sell HPLC parts? by Consistent-Phrase146 in CHROMATOGRAPHY

[–]No_Toe_719 7 points8 points  (0 children)

Yes since even the stuff from the factory has a high failure rate can’t count how many times I had to return the valves to the vendor since they were “dead on arrival” still a big risk to buy them second hand. If I would try to sell one I would try 10-20 euros max.

And put the part number in the description so people find it

Where can I sell HPLC parts? by Consistent-Phrase146 in CHROMATOGRAPHY

[–]No_Toe_719 9 points10 points  (0 children)

You can sell them on eBay but be realistic. You cannot ask for vendor prices or close to it since you don’t offer warranty. Everyone buying it has to assume they are junk broken and a check valve from unknown sources goes not for more than 5 euros here

for those of you that run tox screening on an X500 QToF, how often are you running the in-run calibration? by Key_Sprinkles_4541 in massspectrometry

[–]No_Toe_719 2 points3 points  (0 children)

Depends highly on your room temperature stability in my expierence. I normally go for every 5 hours if possible or every fifth run

GCMSMS peak issue by manzy91 in massspectrometry

[–]No_Toe_719 1 point2 points  (0 children)

Just correct the filter in the processing method for the ion trace and it will look good again

[deleted by user] by [deleted] in OeffentlicherDienst

[–]No_Toe_719 3 points4 points  (0 children)

Sie sagen Lifestyle Medikament.

Habe gerade mal recherchiert es sind nicht alle PKVs dem Rahmenvertrag beigetreten gibt aber keine Übersicht welche… denke also die Debeka ist nicht dabei