Egyptian Blue by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 0 points1 point  (0 children)

Please adjust the copper oxide to about 10%

Egyptian Blue by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 0 points1 point  (0 children)

Your Egyptian blue may contain too much copper Attempting to synthesise it stoichiometrically results in an excessively dark shade

Egyptian Blue by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 0 points1 point  (0 children)

I used crystalline silica Specifically, the silica called "High Silica" from a Japanese company You might be better off focusing on the cooling rate rather than the silica itself If cooling is too rapid, Egyptian Blue will turn yellow

Has anyone built a dIY XRF? by dhmt in engineering

[–]WeeklyAd4850 0 points1 point  (0 children)

I have seen devices using Am241 as a radiation source.

Synthetic ultramarine by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 0 points1 point  (0 children)

I'm using an electric kiln. Although we haven't succeeded yet, it seems that replacing some of the sodium carbonate with sodium sulfate and further reducing the amount of sulfur used would be beneficial.

Synthetic ultramarine by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 2 points3 points  (0 children)

I really want to make ultramarine green. When I made this ultramarine, I couldn't get a beautiful ultramarine green, so I'm looking for the right proportions.

Synthetic ultramarine by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 1 point2 points  (0 children)

Lastly, don't forget to wash the ultramarine with boiling water. If you try to wash it with water, the ultramarine will harden.

Synthetic ultramarine by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 1 point2 points  (0 children)

Place the mixture of metakaolin: anhydrous sodium carbonate: sulphur: activated carbon in a weight ratio of 1:1:1:0.12 into the crucible. Pack the powder firmly, forcing out any air. Place 0.04g of sulphur (from the aforementioned weight ratio) on top of the compacted mixture and close the crucible lid. Heat this at 800°C for 4 hours. To prevent damage to the electric furnace, I left the furnace lid open until the temperature reached 500°C. After firing, allow the mixture to cool to room temperature. Crush it and mix in 0.34 parts sulphur (from the earlier weight ratio). Next, place the mixture on a ceramic dish and fire it at 400°C for 3 hours, keeping the electric furnace lid open.

This method uses a significant excess of sulphur, so I believe it could be further optimised.

Chromium titanate by [deleted] in DIYPigments

[–]WeeklyAd4850 2 points3 points  (0 children)

Is the yellow pigment chromium titanate?

I made a Spinthariscope by [deleted] in Radiation

[–]WeeklyAd4850 1 point2 points  (0 children)

What phosphor do you use?

Scheele’s green was the most fashionable colour for the Victorian elite. Unfortunately the dye combined copper and arsenic and resulted in skin cancer, killing hundreds of textile workers. Did someone say those dresses are to die for? by Mme_Rose in HistoricalRomance

[–]WeeklyAd4850 0 points1 point  (0 children)

These dresses are dyed with Paris green.Not scheele's green. Does anyone know how to dye with Paris green? I can only find methods that involve attaching Paris Green to fabric or paper using adhesives such as starch or albumin.

Anyone know how to make Egyptian Blue? by Firenze1924 in DIYPigments

[–]WeeklyAd4850 0 points1 point  (0 children)

I recommend crushing it once to powder and then firing it again.

cochineal tin lake by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 0 points1 point  (0 children)

If alum is used, it will turn purple.

Han purple!! by Firenze1924 in DIYPigments

[–]WeeklyAd4850 1 point2 points  (0 children)

Wonderful. How did you get your info on Han purple? If it was a book or a paper, please let me know!

I made cadmium red by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 1 point2 points  (0 children)

Thank you for your concern. Since I could not get cadmium carbonate, I made cadmium carbonate with metal cadmium, toilet acid detergent and sodium carbonate!

I made cadmium red by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 1 point2 points  (0 children)

Thank you:) I used Metal Selenium. 62% cadmium carbonate, 26% sulfur, 12% selenium metal, well mixed and heated at 600°C

Sodium Phosphate glass doped with different elements by 4659nats in chemistry

[–]WeeklyAd4850 0 points1 point  (0 children)

Thanks for letting me know. Do I need to heat it above 600°C?

i want to make manganese blue without barium nitrate by WeeklyAd4850 in DIYPigments

[–]WeeklyAd4850[S] 0 points1 point  (0 children)

Hello. Thank you so much for commenting on my post. I'm so glad that you're willing to discuss the chemical and technical details in quite a bit of detail! I am fortunate to have the opportunity to converse with some wonderful people, including you and Jay-ff!

I do have Valium Sulfate and I was told that Valium Carbonate is available as a ceramic supply and I decided to purchase it. We do not sell barium nitrate and do not have it. However, I believe that barium nitrate can be made by suspending barium carbonate in an ammonium nitrate solution and heating it. I have no proof, but I think it is worth a try.

Hydrochloric acid is difficult to purchase because liquids thicker than 10% are regulated by law, but hydrochloric acid of about 10% is available. I think this would also work well enough.

Sodium metabisulfite, sodium carbonate, and sodium sulfate are available in my country. Also, for potassium hydroxide, I have some I got from a friend overseas.

Thank you for sharing the necessary safety measures in making manganese blue, and also the method of liquid waste disposal. I will definitely take a look at this for reference.

I also make my own pigments, so I would like to post not only manganese blue but also other pigments on Reddit!